›› 2013, Vol. 33 ›› Issue (8): 505-508.

• 基础与临床研究 •    下一篇

氧化锆处理剂对氧化锆陶瓷短期粘结强度的影响

谢海峰1,陈晨1,王晓菲1,宋鑫1,章非敏2   

  1. 1. 南京医科大学
    2. 南京医科大学口腔医学院
  • 收稿日期:2012-07-05 修回日期:2012-08-04 出版日期:2013-08-28 发布日期:2013-09-03
  • 通讯作者: 章非敏 E-mail:fmzhang@njmu.edu.cn
  • 基金资助:
    江苏省高校高新技术产业化推广项目;江苏省科技兴卫工程医学领军人才项目

Effects of a new zirconia primer on short-time resin bond strength of zirconia

  • Received:2012-07-05 Revised:2012-08-04 Online:2013-08-28 Published:2013-09-03

摘要: 目的 评价一种新型氧化锆处理剂对氧化锆陶瓷与树脂短期粘结强度的影响。方法加工32个氧化锆瓷块随机分为4组分别对粘结面进行以下处理:组A,氧化铝喷砂;组B,喷砂后硅涂层处理并应用硅烷偶联剂;组C,喷砂并应用包含10-MDP单体的瓷处理剂;组D,喷砂并应用新型氧化锆陶瓷处理剂。制作32枚光固化复合树脂圆柱并用传统Bis-GMA基质的树脂水门汀粘结于预处理后的氧化锆瓷块上,水浴24 h后测试剪切粘结强度并进行断裂模式分析。以扫描电镜和表面能谱分析对处理剂处理的氧化锆进行表征,红外光谱(FTIR)表征处理剂。结果 组A和组D分别显示了最低和最高的粘结强度。结论 新型氧化锆处理剂能够提高氧化锆陶瓷的短期树脂粘结强度。

关键词: 陶瓷, 口腔, 粘结, 氧化锆, 处理剂, Ceramic, Dental, Adhesion, Zirconia, Primer

Abstract: Objective: The aim of the study was to evaluate the effect of a new zirconia primer on bond strength between resin composite and zirconia. Methods: 32 zirconia blocks were manufactured and randomly divided into 4 groups and received different surface-treatments. Group A: alumina sandblasted; Group B: alumina sandblasted followed by silica coating via sol-gel process combined by applying silane couple agent; Group C: alumina sandblasted followed by applying a ceramic primer contained 10-MDP monomer; Group D: alumina sandblasted followed by applying a new zirconia experimental primer. 32 light-cured composite resin cylinders were prepared and bonded on the zirconia discs using a conventional Bis-GMA based resin cement. Then, shear bond strengths (SBS) and modes of failure were determined. Scanning electron microscopy (SEM) and Energy Dispersive X-ray Spectroscopy (EDS) were used for characterization of zirconia treated by the experimental primer, and FTIR was used for characterization of the experimental primer. Results: According to statistical analysis, group A presented the lowest SBS values, while group D presented the highest mean SBS values. Conclusion: Using of the new zirconia experimental primer increases the short-time bond strength of zirconia.

中图分类号: