›› 2015, Vol. 35 ›› Issue (12): 1032-1035.

• 基础研究 • 上一篇    下一篇

H2O2溶液表面处理对纤维桩和树脂水门汀粘接强度的影响

陈兰竹,谢伟丽,孙亚杰,郭彬,李雅静,艾振龙   

  1. 哈尔滨医科大学附属第一医院
  • 收稿日期:2015-04-16 修回日期:2015-05-28 出版日期:2015-12-28 发布日期:2015-12-15
  • 通讯作者: 陈兰竹 E-mail:clz198907@126.com
  • 基金资助:
    黑龙江省科技攻关项目

Effect of H2O2 surface treatments on the bond strength between fiber posts and resin cement

  • Received:2015-04-16 Revised:2015-05-28 Online:2015-12-28 Published:2015-12-15

摘要: 目的 评价不同浓度H2O2溶液表面处理对玻璃纤维桩与树脂水门汀粘接强度的影响。方法 将25支POPO纤维桩随机分成5组:A组(对照组),B组(硅烷组),C组(10% H2O2+硅烷组),D组(20% H2O2+硅烷组),E组(30% H2O2+硅烷组)。将纤维桩与树脂水门汀粘接制作树脂块及薄片试件,将试件放在万能试验机上加载后算出粘接强度,体视显微镜观察破坏模式,统计学分析。结果 各组粘接强度值为:A组 (12.36±1.66)MPa,B组(12.76±1.59)MPa,C组(16.10±2.55)MPa,D组(19.19±2.81)MPa,E组(21.95±2.95) MPa。5组数据两两比较,除AB组比较无统计学意义(P>0.05),其余均有统计学意义(P<0.05)。结论 仅用硅烷偶联剂对玻璃纤维桩进行表面处理的粘接强度并未提高;H2O2溶液处理后再涂硅烷偶联剂可提高玻璃纤维桩与树脂水门汀的粘接强度,随H2O2溶液浓度的增加,粘接强度增加增多。

关键词: 纤维桩, H2O2, 树脂水门汀, 表面处理, 硅烷化

Abstract: Objective To evaluate the effect of H2O2 surface treatments on the bond strength between fiber posts and resin cement.Methods 25 POPO glass fiber posts were randomly separated into five groups: Group A (control; no treatment),Group B (silanization),Group C (etching with 10% H2O2 and silanization),Group D (etching with 20% H2O2 and silanization),Group E (etching with 30% H2O2 and silanization).The posts were positioned into a mold to allow adhesive resin cement to be inserted,and to form resin blocks.Then resin block was cut to obtain 1mmthick specimens.The pushout tests were done at a crosshead speed of 0.5 mm/min with a universal testing machine until failure occurred and data were analyzed using oneway ANOVA.The failure mode of each specimen was observed with stereomicroscope.Results The micropushout bond strength values of fiber post from group A to group E: (12.36±1.66) MPa,(12.76±1.59) MPa,(16.10±2.55) MPa,(19.19±2.81) MPa,(21.95±2.95) MPa.Significant difference (P<0.05) was found between each two groups except for Group A and Group B (P>0.05).Conclusions Silanization as the only surface treatment did not improve the bond strength,but the combination of H2O2 and silanization can enhance the bond strength,and with the concentration increased,the bond strength increased.

Key words: fiber post, H2O2, resin cement, surface treatment, silanization 

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