›› 2016, Vol. 36 ›› Issue (2): 116-119.

• 基础研究 • 上一篇    下一篇

不同偶联剂和粘接剂对烤瓷瓷面与金属托槽抗剪切强度影响的体外研究

丁宏1,吴建勇2   

  1. 1. 大连市口腔医院
    2. 南昌大学附属口腔医院
  • 收稿日期:2015-03-06 修回日期:2015-04-22 出版日期:2016-02-28 发布日期:2016-02-29
  • 通讯作者: 吴建勇 E-mail:wjyyrx@163.com

The vitro study of the influence of different silane coupling agents and adhesive materials on shear bond strength of metal brackets to porcelain surface

  • Received:2015-03-06 Revised:2015-04-22 Online:2016-02-28 Published:2016-02-29

摘要: [摘要] 目的 研究不同类型硅烷偶联剂和粘接剂对烤瓷瓷面与金属托槽之间抗剪切强度的影响。方法 将90个烤瓷瓷面行水砂纸打磨去釉,HF酸蚀处理,根据硅烷偶联剂的不同随机分为甲乙丙3组,再根据使用粘接剂不同每组下分3小组,分别用3种不同粘接剂,将90个金属托槽粘接于烤瓷瓷面,托槽粘结60 min后经37 ℃恒温人工唾液水浴孵化24 h,使用Instron万能材料力学试验机测定样本抗剪切强度。结果 使用硅烷偶联剂组抗剪切强度比未使用硅烷偶联剂组大(P<0.05);2种硅烷偶联剂组之间抗剪切强度差异无显著性(P>0.05);光固化复合树脂粘接剂组抗剪切强度大于其他粘接剂组(P<0.05);未使用硅烷偶联剂组瓷面破损指数明显小于使用硅烷偶联剂组(P<0.05)。结论 硅烷偶联剂能有效增加烤瓷瓷面和金属托槽之间的抗剪切强度,光固化复合树脂粘接剂与双组份硅烷偶联剂合用可获得最大的抗剪切强度。

关键词: 抗剪切强度, 硅烷偶联剂, 瓷面粘接

Abstract: Objective: To investigate the influence of different silane coupling agents and different adhesive materials to the shear bond strength of metal brackets bonded to porcelain surface. Methods: 90 porcelain specimens were deglazed by 1000 grit water sandpaper and etched with 9.6%HF acid for 120s, rinsed with distilled water and dried before applying the silane primer. All specimens were divided randomly into 3 groups according to different silane coupling agents application, Each group was subdivided into 3 subgroups depending on different adhesive material, every subgroup had 10 porcelain facets. 90 metal brackets were bonded to ceramic specimens with 3 adhesive material. All specimens were stored in artificial saliva bath at 37℃ for 24 hours. after brackets bonded for 60min, then the specimens were underwent shear testing with Instron universal testing machine. Results: The shear bond strength of the groups treated with silane primer were higher than that without silane primer (p<0.05). There was not any statistically significant in the shear bond strength between the group of one-mix silane coupling agent and the group of two-mix silane coupling agent (p>0.05). The shear bond strength of the group with light-cured composite resin was higher than the others (p<0.05). The groups treated without silane coupling agent showed lower porcelain fracture than the groups treated with silane coupling agent. Conclusions: Silane coupling agent can improve the shear bond strength between metal brackets and porcelain surface. The group of light-cured composite resin treated with two-mix silane coupling agent can get the highest shear bond strength.

Key words: shear bond strength, silane coupling agent, porcelain bonding